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Great difficulty was experienced in obtaining uniformly thick films. The methods of determination of thinner films described in Chapter II gave erratic results. However, the absence of a change of slope in Figure 12 indicates that when water vapor is present the layer of phthalic anhydride, suggested earlier, does not form and the degradation continues at the same rate. All subsequent irradiation experiments employed this holder. A final point in favor of the use of infrared analysis is the transparency of titanium IV oxide pigment in the region of interest. To further eliminate errors due to solvent absorption, a cell of approximately the same thickness as the sample cell was filled with the solvent mixture and placed in the reference beam of the spectrophotometer. Patent 1, , Jan.
Films stored under the conditions of irradiation but shielded from ultraviolet irradiation showed only slight degradation. Although the initial cleavage is photolytic in nature, subsequent reactions of the thermal type seem to occur making the rate of the entire process dependent on temperature. The solution of resin was then placed dropwise on sodium chloride disks 25 mm. On the assumption that much of this scattering was the result of non-reproducible positioning of the samples on the spectrophotometer, a new sample holder was con structed which largely eliminated this source of error. Especially is he grateful to Dr. The first, ori g in a lly postulated by Renz in , 2 1 attributes the decomposition of the film to a cyclic oxidation-reduction process involving the pigment. Phthalic anhydride and the resin showed less association in solution than did phthalic acid and there fore more concentrated solutions of the anhydride and resin could be used.
Resin A was sufficiently soluble in pure chloroform to permit its use as a solvent. This is not to say that subsequent reactions in the overall eesin process are not of the thermal type.
The University of Florida George A. It was first observed after about 90 hours of irradiation. Since it was desired to correlate these infrared data, if possible, with data published on evolution of gases from the films, Experiment I was repeated at a higher temperature, 75 2C.
On the assumption that much of this scattering was the result of non-reproducible positioning of the samples on the spectrophotometer, a new sample holder was con structed which largely eliminated this source of error. The principal degradation product was identified as phthalic anhydride.
The number of fringes and the wave lengths between which they are observed are related to cell thickness by the equation b n X 1 X2 where b is cell thickness in microns and n is the number of fringes observed between the wave lengths. PAGE 31 After about 5 hours of irradiation a new band appeared at 5.
The change of slope near 50 hours, it is felt, indicates the build-up of a layer of phthalic anhydride on the surface of the film.
Renz showed that titanium iV oxide reacts photochemically with glycerol, alkyc carbon dioxide and titanium III oxide. Having earlier observed a radical difference in the rate of anhydride formation when the atmosphere surrounding the samples during irradiation was changed from water saturated oxygen to dry nitrogen, experiments were conducted which were intended to separate, if possible, the effects of water vapor and oxygen on the rate of degradation.
In the case of the anhydride a solution of 20 per cent diethyl ether and 80 per cent chloroform was used. PAGE 24 18 Measurement of Film Thickness In an effort to evaluate the relative thicknesses theis the films being irradiated, three different methods were employed. Any reuse of this item in excess of fair alktd or other copyright exemptions requires permission of the copyright holder.
The first, originally postulated by Renz in21 attributes the decomposition of the film to a cyclic oxidation-reduction process involving the pigment. The mixed solvent systems described in Chapter II give excellent results in the carbonyl region. This has the effect of shifting the carbonyl absorption to shorter wave lengths as one proceeds through the series: Calcium fluoride Slit Program: An enlarged view of this holder is shown in Figure 3.
The carbonyl region of the phthalic anhydride is reproduced in Figure 5.
A study of some factors affecting the degradation of alkyd resins
Degradation of Ester Carbonyl in Moist Air at 30c. Swern, Daniel, et al.
The ready availability of calcium fluoride optics provides much better resolution in the micron region than is available with sodium chloride optics, allowing the accuracy of the instrument to be used to the greatest advantage. The preceding three experiments had all been carried out on Resin A which contained no pigment hhesis drier.
This method has, on occasion, been successful when films were cast on the surface of a pool of water or mercury and allowed to harden. Gropp for continuing advice, assistance, and ins p iration. A set of films of Resin A was irradiated in a nitrogen atmosphere which thessis saturated with water. Later another film sample was prepared in the same manner and stored for 90 hours in air at C.
A study of some factors affecting the degradation of alkyd resins
The resin used was an unmodified glycerol phthalate which will be designated as Resin A throughout the remainder of this paper. The increase in anhydride concentration, and simultaneous decrease in ester concentration, was interpretated as an example of pseudo first order kinetics in photons of ultraviolet light of the required energy for bond cleavage. At this temperature, the thinner film was rapidly akyd to the extent that the carbonyl band at 5.
Great thsis was experienced in obtaining uniformly thick films. In manufacture of phthalic anhydride by the oxidation of naphthalene was begun and products made from this formerly expensive chemical assumed new commercial attractiveness.
Gropp for continuing advice, assistance, and inspiration. Determination of Molar Absorptivity of Phthalic Anhydride
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Case Study: Omni American Bank Takes on Data Loss Prevention
The additional context offers visibility into compliance and policy violations as well as helps distinguish between legitimate business and employee error. Being able to have the visibility of data and controlling what end users were doing has been vital in our rollout.
Operational efficiency with minimal impact on endpoint, options to run when ideal or not using battery, and multiple operating modes includes caze and interactive Accurate identification of confidential data with a comprehensive set of technologies.
As part of her role she developed infosec policy, developed new awareness testing and led the company’s incident stuy team. Introduction This case study of a medium enterprise health care company is based on a June survey of Forcepoint Next Generation Firewall customers by TechValidate, a 3rd-party research service.
Identifies the following as the capabilities that carried the most weight when they chose to migrate to Forcepoint Secure Web Gateway: The State of Web Application Firewalls. Unlike competitive solutions that focus only on what confidential data is being lost and how over Web or emailWebsense Data Monitor is the only solution to automatically provide context to identify what customer data is at risk; who is using the data in real time; and where this data is going over the Web.
However, Kafka is proving to be a disappointment. Rates Forcepoint Web Security Cloud as very effective.
Documentation is already expected and now the bank can give printouts showing how it is protecting data with the solution. Omni American found that the majority of end users outside of the IT area didn’t have a good understanding of data security and so has started actively educating its employees on the reasons why the bank is using the DLP solution to track data.
Company Profile The company featured in this case study asked to have its name publicly blinded because publicly endorsing vendors is against their policies. This comprehensive data loss prevention solution helps protect both her employer and Miss Bea Haven from actions that may be well intended but that could cause unintended security risks. The system has helped us protect customers. Best in class Ease of use: Achieved the following results after using Forcepoint Web Security Cloud: Rates Forcepoint Secure Web Gateway as very scalable for their company.
Top 5 Health Data Breaches. Discovery and classification of all confidential data on endpoint. Sign in with your ISMG account. The Websense Data Endpoint security module offers: Chose Forcepoint because of the following capability: This case study of a medium enterprise financial services company is based on a June survey of Forcepoint CASB customers by TechValidate, a 3rd-party research service.
webswnse It wasn’t a hard decision to make, the solution we chose allows us to monitor and manage the solution centrally. Learn the fundamentals of developing a risk management program from the man who wrote the book on the topic: Superior Ease of use: Developing a Comprehensive Mobile Security Strategy.
Identify and Monitor Confidential Data on the Network
The profiled company asked to have their name blinded to protect their confidentiality. Lower Total Cost of Ownership Reports that their end-user internet performance significantly improved as a result of moving to the Forcepoint Next Generation Websese. Getting Past the ‘Fake News’.
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